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- W2352381402 abstract "The title compound was prepared from 3,4,5-trimethoxytoluene (THT) by Vilsmeier-Haack reaction. THT was dissolved in DMF, added dropwise to phosphorous oxychloride, reacted at 60℃~70 ℃for 8-10 hours, then neutralized with 10% NaOH to give the product. Yield was 92.23%, purity, 98.8%, and melting point, 61℃~64℃. The effect of reaction conditions on yield and purity of the product was studied, and the product was characterized." @default.
- W2352381402 created "2016-06-24" @default.
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- W2352381402 date "2003-01-01" @default.
- W2352381402 modified "2023-09-25" @default.
- W2352381402 title "Preparation of 6-Methyl-2,3,4-trimethoxybenzaldehyde" @default.
- W2352381402 hasPublicationYear "2003" @default.
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