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- W2352427474 abstract "The liquid crystalline compound, 2,6-bis(benzylidene)cyclohexanone was synthesized using benzal-dehyde and cyclohexanone as raw materials, and tetrabutyl ammonium bromide as phasetransfer catalyst in the solution of sodium hydroxide. Effect of many factors, such as reaction time, reaction temperature and concentration of sodium hydroxide, was studied. The product was confirmed by IR, 1H-NMR and element analysis. The liquid crystalline behavior of compound was studied by DSC, optical polarizing micrographs and wideangle X-ray diffraction. The experimental results show that the synthesized compound exhibits typical semectic thermot ropic liquid crystal. Meanwhile, the crystal of compound was determined by X-ray single-crystal diffraction. The crystal of the compound belongs to monoclinic system with space group P2(1)/c, a=9.586(1), b = 18.391(2), c = 9.433(1), α = 90°, β =115.816(2) °, γ = 90°, Dc = 1.217 g.cm-3, V = 1496.9(3) -3, and Z = 4." @default.
- W2352427474 created "2016-06-24" @default.
- W2352427474 creator A5059696161 @default.
- W2352427474 date "2009-01-01" @default.
- W2352427474 modified "2023-09-22" @default.
- W2352427474 title "Synthesis of 2,6-bis(benzylidene)cyclohexanone and study of liquid crystal Behavior" @default.
- W2352427474 hasPublicationYear "2009" @default.
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