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- W2352673357 abstract "A new,simple and sensitive method for simultaneous separation of two pairs of anisodamine enantiomers has been firstly developed and validated using CZE in combination with partial filling technique and field-amplified sample injection.Carboxymethylated-β-cyclodextrins(CM-β-CD) was used as chiral selector in this system.Effects of pH,CM-β-CD content,filling time of separation buffer,and separation voltage on the enantiomer separation behavior were evaluated.In an optimal condition,the four enantiomers were resolved in 23 min by partially filling an electrophoretic capillary with 1.7% CM-β-CD(1.0psi,90 s) and carrying out an electrophoresis with 75 mmol·L-1 Tris-H3PO4(pH 3.5) at 17.5 kV.The sensitivity was further improved by field-amplified sample injection(0.2psi,1.5s water plug).Real sample was also tested and promising results for the determination of anisodamine enantiomers were obtained." @default.
- W2352673357 created "2016-06-24" @default.
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- W2352673357 date "2012-01-01" @default.
- W2352673357 modified "2023-09-22" @default.
- W2352673357 title "Chiral Separation & Quantification of Anisodamine by CE Coupling with Partial Filling Technique & Field-amplified Sample Injection" @default.
- W2352673357 hasPublicationYear "2012" @default.
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