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- W2352807400 abstract "Based on derivative reaction,a new derivative fluorescence method is developed for the determination of sibutramine hydrochloride.The derivative system,reaction conditions and stability of the products were studied in detail.It is assured that the mixture of acetic anhydride and malonic acid react with sbutramine hydrochloride for 15 min at 75 ℃,the product has highly fluorescence at λ_(ex)=456 nm and λ_(em)=496 nm.In the selected conditions,the fluorescence intensity was linearly related to concentration of sibutramine hydrochloride in the range of 0.11～9.5 μg/mL,the detection limit of 13.4 ng/mL,the recovery is 95.4%～104.2%.The method is applied to the determination of sibutramine hydrochloride in qumei capsules,with satisfactory results." @default.
- W2352807400 created "2016-06-24" @default.
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- W2352807400 date "2006-01-01" @default.
- W2352807400 modified "2023-09-25" @default.
- W2352807400 title "Determination of sibutramine hydrochloride by derivative fluorescence spectroscopy" @default.
- W2352807400 hasPublicationYear "2006" @default.
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