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- W2352807526 abstract "Dichloroacetaldehyde, an intermediate of organic insecticide, can be synthesized by the catalytic chlorination of paraldehyde or aldehyde. The selection of catalysts, the temperature of various stages of the reaction, etc., were investigated and dichloroaldehyde was obtained in good yields.The experimental results indicate that antimony trichloride is more active than sulfur for catalytic chlorination of paraldehyde or aldehyde. It is necessary to control the reaction temperature, the quantity of catalyst and the molar ratio of the reactants accurately. The product, containing 90~95% of dichloroacet-aldehyde, was obtained in 75~78% yields.Formation of tarry distillation residue due to the polymerization increases with the increasing of the reaction temperature or the quantity of antimony trichloride." @default.
- W2352807526 created "2016-06-24" @default.
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- W2352807526 date "1965-01-01" @default.
- W2352807526 modified "2023-09-24" @default.
- W2352807526 title "SYNTHESIS OF DICHLOROACETALDEHYDE BY CATALYTIC CHLORINATION OF PARALDEHYDE" @default.
- W2352807526 hasPublicationYear "1965" @default.
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