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- W2353651788 abstract "OBJECTIVE To eastablish a method for the determination of residual organic solvents in Doxepin Hydrochloride by capillary gas chromatography.METHODS The GC determination was performed on 100%Polydimethylsiloxane(30.0m×320μm×0.4μm)with FID detection.The injection port temperature was maintaining at 220℃ and the detector temperature was maintaining at 250℃.The initial column temperature was 30℃,maintaining it for 14min,then raising the temperature to 85℃ at the rate of 30℃/min,maintaining it for 2min,last raising the temperature to 180℃ at the rate of 50℃/min,maintaining it for 2min.N2 is the carry gas,the initial flow rate was 0.7mL·min-1,maintaining it for 14min,then raising the flow rate to 2mL·min-1 at the rate of 1mL·min-1,maintaining it for 7.7min.RESULTS Under experiment condition,seven residual organic solvents were separated thoroughly.Every solvents have good linear relationship and recovery.None of residual organic solvent was found to exceed quality limit.CONCLUSION The method is proved to be simple and accurate.It is suitable for determination of organic solvents in Doxepin Hydrochloride." @default.
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- W2353651788 date "2011-01-01" @default.
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- W2353651788 title "Determination of residual organic solvents in Pioglitazone Hydrochloride by capillary gas chromatography" @default.
- W2353651788 hasPublicationYear "2011" @default.
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