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- W2353791559 abstract "Ceftiofur related residues in bovine and porcine muscle and kidney were determined by high performance liquid chromatography.Samples were extracted with dithioerythritol,derivatized with iodoacetamide and cleaned up on C18,SAX and SCX solid-phase extraction cartridges.Chromatographic separation was carried out on a C18 column(250 mm×4.6 mm,5 μm) with acetonitrile-water(15 ∶85 by volume) containing 0.1% trifluoroacetic acid as mobile phase at a flow rate of 1 mL/min,followed by determination of the residue by ultraviolet absorption detector at 266 nm.Calibration curve was linear between 0.016 and 1.28 mg/L,with the correlation coefficient r0.999 9.The recovery and relative standard deviation ranged from 90%to 91%and 1.8%to 3.5%at spiked level of 200-8 000 μg/kg,respectively.The detection limit of the proposed method was 50 μg/kg." @default.
- W2353791559 created "2016-06-24" @default.
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- W2353791559 date "2008-01-01" @default.
- W2353791559 modified "2023-09-28" @default.
- W2353791559 title "Determination of Ceftiofur Related Residues in Bovine and Porcine Muscle and Kidney by High Performance Liquid Chromatography" @default.
- W2353791559 hasPublicationYear "2008" @default.
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