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- W2354145466 abstract "Objective:To develop an HPLC method for determination of narigin,hesperidin and neohesperidin in Muxiang Fenqi Pill.Method:The analysis was carried out with an Agilent C18(4.6 mm×250 mm,5μm)column and the mobile phase of acetonitrile-1% phosphoric acid(21∶79).The flow rate was 1.0 mL · min-1 and column temperature was 30 ℃.The detection wavelength was set at 283 nm.Result: The calibration curve was linear within the range of 0.110 8-1.218 8 μg(r=0.999 4,n=6),0.226 8-2.494 8 μg(r=0.999 7,n=6)and 0.084 8-0.932 8 μg(r=0.999 4,n=6) for narigin,hesperidin and neohesperidin.The average recoveries were 97.5%(RSD 0.80%,n=6),99.0%(RSD 1.7%,n=6) and 98.2%(RSD 1.6%,n=6) respectively.Conclusion:The results showed this method is reproducible,sensitive and accurate for determination of narigin,hesperidin and neohesperidin in Muxiang Fenqi Pill." @default.
- W2354145466 created "2016-06-24" @default.
- W2354145466 creator A5066853549 @default.
- W2354145466 date "2012-01-01" @default.
- W2354145466 modified "2023-09-23" @default.
- W2354145466 title "Determination of Narigin,Hesperidin and Neohesperidin in Muxiang Fenqi Pill by HPLC" @default.
- W2354145466 hasPublicationYear "2012" @default.
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