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- W2354408963 abstract "Objective To develop a method for the determination of sinomenine and rhein in Tongfeng capsule.Methods The assay of sinomenine was performed on Agilent Eclipse Plus C18 column(5 μm,4.6 mm×250 mm) with a DAD(262 nm).The mobile phase was acetonitrile-0.08% triethylamine(21:79) with a flow rate of 1.0 mL·min-1.The determination of rhein was on a Kromasil C18 column(5 μm,4.6 mm×250 mm) with a UVD(254 nm).The mobile phase was methanol-0.05% phosphoric acid(85:15).Results The linear range of sinomenine was 0.115 6-3.855 μg(r=0.999 5),and the average recovery ratio was 99.48%(RSD=1.93%);The linear range of rhein was 0.083 2-0.832 μg(r=0.999 5),and the average recovery ratio was 98.62%(RSD=1.13%). Conclusion The method is exclusive,accurate and reproducible,which may be applied in the quality control of Tongfeng capsule." @default.
- W2354408963 created "2016-06-24" @default.
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- W2354408963 date "2012-01-01" @default.
- W2354408963 modified "2023-09-28" @default.
- W2354408963 title "Determination of sinomenine and rhein in Tongfeng capsules by HPLC" @default.
- W2354408963 hasPublicationYear "2012" @default.
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