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• W2355983232 endingPage "72" @default.
• W2355983232 startingPage "67" @default.
• W2355983232 abstract "Multicomponent crystallization of l-tryptophan with three different isomers of pyridinedicarboxylic acids, namely, 2,3-pyridinedicarboxylic acid (2,3-PDA), 2,5-pyridinedicarboxylic acid (2,5-PDA) and 2,6-pyridinedicarboxylic acid (2,6-PDA), were screened using conventional solution cocrystallization technique. Whereas the new phases derived from the amino acid with 2,3-PDA or 2,5-PDA were analyzed using powder X-ray diffraction and thermal analysis techniques, the crystalline phase synthesized from 2,6-substituted isomer was further characterized by single crystal X-ray diffraction. Structural analysis revealed that the amino acid exists in the zwitterionic form interacting with the neutral 2,6-PDA by strong intermolecular hydrogen bonding. The components in the co-crystal self-assemble leading to a three dimensional hydrogen bonded closed packed network structure. Isothermal calorimetric titration showed that among the three isomers, 2,6-PDA showed relatively strong binding interaction towards the amino acid in water at 298 K. All the crystals exhibit marginal quenching of fluorescence properties of l-tryptophan in the solid state." @default.
• W2355983232 created "2016-06-24" @default.
• W2355983232 creator A5057815706 @default.
• W2355983232 date "2016-08-01" @default.
• W2355983232 modified "2023-09-26" @default.
• W2355983232 title "Screening of multicomponent crystals of l -tryptophan with three isomers of pyridinedicarboxylic acids" @default.
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• W2355983232 doi "https://doi.org/10.1016/j.jcrysgro.2016.05.009" @default.
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