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- W2356552233 abstract "The cyanoethylated bamboo powder was prepared with bamboo powder and acrylonitrile by microwave irradiation after ultrasonic activated.The effects of formula and reactive condition on the cyanoethylation were studied and the products were characterized by electro microscope,X-ray diffraction(XRD),Fourier transform infrared(FTIR) spectroscope and differential scanning calorimeter(DSC)etc.The optimal formula and reactive condition were that 1.5 g of bamboo powder was pretreated by ultrasonic for 10 min in saturated KSCN solution contained 1 mol·L-1 of NaOH,then reacted with 8 mL of acrylonitrile by microwave irradiation at the temperature of 40 ℃.The same weight gain ratio(about 40%) could be obtained by conventional water bath method,but the reaction time was prolonged from the primary 30 min to 180 min.Cyanoethylation could be completed at the mild condition and short time which could reduce the side reaction of acrylonitrile as hydrolyzation and homopolymerization.The structure of cellulose of cyaoethylated bamboo powder was distroyed and the surface of product became rough.The bundle of fibre and the crystallinity of cellulose decreased and a new endothermic peak between 145 ℃ and 290 ℃ appeared." @default.
- W2356552233 created "2016-06-24" @default.
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- W2356552233 date "2012-01-01" @default.
- W2356552233 modified "2023-09-24" @default.
- W2356552233 title "Preparation and Characteristic of Cyanoethylated Bamboo Powder by Microwave Irradiation" @default.
- W2356552233 hasPublicationYear "2012" @default.
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