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- W2356559630 abstract "The cis/trans-4-tert-butylcyclohexanols were synthesized with 4-tert-butylphenol via catalytic hydrogenation.With appropriate amount tert-butyl dimethyl chlorosilane(TBDMSCl),more than 99.5%purity of cis-4-tert-butylcyclohexanol could be obtained by derivatization method.The results of hydrogenation condition experiments showed the reaction effect was best when the amount of concentrated hydrochloric acid was 0.25 g,isopropanol as solvent and the reaction temperature was 70～80 ℃.The reaction mechanism of cis/trans-4-tert-butylcyclohexanols separation was speculated according to the derivatization data." @default.
- W2356559630 created "2016-06-24" @default.
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- W2356559630 date "2012-01-01" @default.
- W2356559630 modified "2023-09-26" @default.
- W2356559630 title "Synthesis of high purity cis-4-tert-butylcyclohexanol by derivatization method" @default.
- W2356559630 hasPublicationYear "2012" @default.
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