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- W2356584974 abstract "Glycidol was synthesized through the reaction of 3-chloro-1,2-propanediol with alkaline compound at low temperature.When the dosage of 3-chloro-1,2-propanediol was 2 mol,with 500 mL isopropanol as solvent,the reaction was kept running at 0 ℃ for 90 min on dropping w(NaOH)=37% aqueous solution.Anhydrous magnesium sulfate was added as desiccant 50 min after the beginning of reaction in order to absorb the overfull water.The structure of glycidol was confirmed by IR and 1HNMR.The refractive index(n20D),epoxide value(Ev) and boiling point of the product are very close to those of standard sample(CAS No.556-52-5).The yield of the reaction is 82.5% under the optimal conditions." @default.
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- W2356584974 date "2007-01-01" @default.
- W2356584974 modified "2023-09-27" @default.
- W2356584974 title "Synthesis and Characterization of Glycidol" @default.
- W2356584974 hasPublicationYear "2007" @default.
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