Matches in SemOpenAlex for { <https://semopenalex.org/work/W2356659063> ?p ?o ?g. }
Showing items 1 to 69 of
69
with 100 items per page.
- W2356659063 abstract "Objective: To establish a supplemental test method to identify illegally added paracetamol in Tianma capsules.Methods: Rapid screening was performed by TLC method.HPLC-PDA was adopted to conduct the quantitative inspection,the column was Polaris C18(4.6 mm × 250 mm,5 μm),the mobile phase was methanol 0.6% acetic acid(10∶ 90) at a flow rate of 1.0 mL min-1 with a detection wavelength of 243 nm,the column temperature was 30 ℃.IR method was used for rapid identification with UPLC-MS method for the structural confirmation;the column was Acquity UPLC BEH C18(50 mm × 2.1 mm × 1.7 μm),the mobile phase was 0.1% formic acid-acetonitrile(5∶ 95) at a flow rate of 0.4 mL.min-1.Mass conditions were set in a positive ion mode for detection with electrical ionization source(ESI),the source voltage of 3.1 kV,the capillary temperature of 400 ℃,the cone voltage of 30 V,the sheath gas flow rate of 600 L.h-1,using first-order full scan and second-order full-scan modes,the mass range was from 50 to 1000.Results: TLC method is simple,rapid,specific,which can be used for rapid screening;HPLC-PDA method can accurately detect the content of acetaminophen,by which there were 3 batches detected in five batches of samples and 2 batches not detected;UPLC-MS method for structural confirmation is highly characteristic and accurate.Conclusion: The method is confirmatory,highly sensitive and applicable to detect illegal added paracetamol in Chinese patent medicines." @default.
- W2356659063 created "2016-06-24" @default.
- W2356659063 creator A5012937416 @default.
- W2356659063 date "2013-01-01" @default.
- W2356659063 modified "2023-09-25" @default.
- W2356659063 title "Method for supplemental test of paracetamol in quality standard of Tianma capsules" @default.
- W2356659063 hasPublicationYear "2013" @default.
- W2356659063 type Work @default.
- W2356659063 sameAs 2356659063 @default.
- W2356659063 citedByCount "0" @default.
- W2356659063 crossrefType "journal-article" @default.
- W2356659063 hasAuthorship W2356659063A5012937416 @default.
- W2356659063 hasConcept C113196181 @default.
- W2356659063 hasConcept C121332964 @default.
- W2356659063 hasConcept C162356407 @default.
- W2356659063 hasConcept C172120300 @default.
- W2356659063 hasConcept C178790620 @default.
- W2356659063 hasConcept C179998833 @default.
- W2356659063 hasConcept C185592680 @default.
- W2356659063 hasConcept C2776673659 @default.
- W2356659063 hasConcept C2777379063 @default.
- W2356659063 hasConcept C2777463227 @default.
- W2356659063 hasConcept C2779607525 @default.
- W2356659063 hasConcept C40684141 @default.
- W2356659063 hasConcept C43617362 @default.
- W2356659063 hasConcept C55493867 @default.
- W2356659063 hasConcept C62520636 @default.
- W2356659063 hasConceptScore W2356659063C113196181 @default.
- W2356659063 hasConceptScore W2356659063C121332964 @default.
- W2356659063 hasConceptScore W2356659063C162356407 @default.
- W2356659063 hasConceptScore W2356659063C172120300 @default.
- W2356659063 hasConceptScore W2356659063C178790620 @default.
- W2356659063 hasConceptScore W2356659063C179998833 @default.
- W2356659063 hasConceptScore W2356659063C185592680 @default.
- W2356659063 hasConceptScore W2356659063C2776673659 @default.
- W2356659063 hasConceptScore W2356659063C2777379063 @default.
- W2356659063 hasConceptScore W2356659063C2777463227 @default.
- W2356659063 hasConceptScore W2356659063C2779607525 @default.
- W2356659063 hasConceptScore W2356659063C40684141 @default.
- W2356659063 hasConceptScore W2356659063C43617362 @default.
- W2356659063 hasConceptScore W2356659063C55493867 @default.
- W2356659063 hasConceptScore W2356659063C62520636 @default.
- W2356659063 hasLocation W23566590631 @default.
- W2356659063 hasOpenAccess W2356659063 @default.
- W2356659063 hasPrimaryLocation W23566590631 @default.
- W2356659063 hasRelatedWork W2252352437 @default.
- W2356659063 hasRelatedWork W2349476412 @default.
- W2356659063 hasRelatedWork W2354460924 @default.
- W2356659063 hasRelatedWork W2358670877 @default.
- W2356659063 hasRelatedWork W2359427203 @default.
- W2356659063 hasRelatedWork W2359594554 @default.
- W2356659063 hasRelatedWork W2359632065 @default.
- W2356659063 hasRelatedWork W2361169319 @default.
- W2356659063 hasRelatedWork W2363684100 @default.
- W2356659063 hasRelatedWork W2364958983 @default.
- W2356659063 hasRelatedWork W2370417132 @default.
- W2356659063 hasRelatedWork W2371201420 @default.
- W2356659063 hasRelatedWork W2376802459 @default.
- W2356659063 hasRelatedWork W2383707545 @default.
- W2356659063 hasRelatedWork W2385246786 @default.
- W2356659063 hasRelatedWork W2387332135 @default.
- W2356659063 hasRelatedWork W2388787737 @default.
- W2356659063 hasRelatedWork W2389296730 @default.
- W2356659063 hasRelatedWork W2392538450 @default.
- W2356659063 hasRelatedWork W2393935511 @default.
- W2356659063 isParatext "false" @default.
- W2356659063 isRetracted "false" @default.
- W2356659063 magId "2356659063" @default.
- W2356659063 workType "article" @default.