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- W2356702912 abstract "In the analysis, brass sample, in the form of rod, cubes chips or granules was used as the anode, and Pt gauze electrode as the cathods, and dissolution of the sample was performed by electrolysis, during which cupric ions were reduced and plated on the Pt cathode. Copper content of the sample was determined by electro-gravimetry. Amount of sample dissolved by the electrolytic method was calculated by the formula given in the paper. Appropriate amount of conc. HCl was added to the electrolyte to make it 0.1 mol·L~(-1) in H_2SO_4, 0.05 mol·L~(-1) in HNO_3 and 1.0 mol·L~(-1) in HCl, and its volume was made up to 200 mL. An aliquat of the solution having its zinc content around 60 mg, was taken and passed through an ion-exchange column packed with an ion exchange resin to adsorb the zinc in the form of ZnCl~(2-)_4. The effluent solution from the column was used for ICP-AES determination of other alloying elements and also the impurity elements. Dilute nitric acid of 0.1 mol·L~(-1) was used as eluant to desorb the ZnCl~(2-)_4 from the resin and determined by EDTA titration. Three CRM′s of brass were analyzed by the proposed method, and results in consistency with the certified values were obtained. Discussion and optimization of analytical conditions and parameters were also given." @default.
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- W2356702912 date "2005-01-01" @default.
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- W2356702912 title "ICP-AES ANALYSIS OF BRASS WITH ELECTROLYTIC SAMPLE-DISSOLUTION" @default.
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