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- W2356923218 abstract "Simultaneous determination of five speciations of arsenic compounds including arsenite,arsenate,monomethylarsonic acid,dimethylarsinic acid,and roxarsone was studied by liquid chromatography-hydrodide generation-atomic flurescence spectrometry.It was showed that five speciation of arsenic compounds could be separated through C18 reversed phase column using NaH2PO4:CH3OH solution containing 0.5 mmol/L tetrabutyl ammonium bromide as mobile phase at the gradient elution condition;Arsenic compounds could form optimal fluorescence signal using 20 g/L K2S2O8 as UV digest oxidant,7% hydrochloric acid as carrying solution and 20 g/L KBH4 solution as reducing agent.A good linear relationship between fluorescence peak area and concentration of five kinds of arsenic compounds in certain range was obtained.The detection limit of arsenic compounds was not more than 10.0 μg/L,recoveries were controlled in the range of 81.4%-105.6% and relative standard deviations less than 4.0%.This method can be applied to analyze the concentration of roxarsone and its metabolites such as arsenite,arsenate,monomethylarsonic acid,dimethylarsinic acid in feed,chicken manure,soil and plant samples." @default.
- W2356923218 created "2016-06-24" @default.
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- W2356923218 date "2010-01-01" @default.
- W2356923218 modified "2023-09-25" @default.
- W2356923218 title "Simultaneous Analysis of Roxarsone and Its Metabolites by Liquid Chromatography-Hydrodide Generation-Atomic Fluorescence Spectrometry" @default.
- W2356923218 hasPublicationYear "2010" @default.
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