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- W2357049069 abstract "1-Hydroxy benzotriazole was synthesized by O-chloronitrobenzene and hydrazine hydrate using PEG-800 as phase transfer catalyst. Various reaction factors influencing the yield of the target product were discussed. The optimum reaction conditions were as follows:the molar ratio of O-chloronitrobenzene, hydrazine hydrate to PEG-800 was 1∶4∶0.03, the speed of agitator 500 r/min,the reaction time 5 h,the reaction temperature 110℃. The yield reached 98.1% under these optimum conditions." @default.
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- W2357049069 date "2007-01-01" @default.
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- W2357049069 title "Synthesis of 1-Hydroxy Benzotriazole by Phase-transfer Catalysis" @default.
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