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- W2357788219 abstract "p-Methylphenyl 2,3-anhydro-4,6-o-benzylidene-1-thio-β-D-allopyranoside (Ⅲ) has been prepared from p-methylphenyl 4,6-o-benzylidene-1-thio-β-D-glucopyranoside (Ⅰ). The difference in activity between 2-OH and 3-OH for the tosylation reaction has been explored. Orthogonal experiments in the temperature range of -10～60°C and in the Ⅰ and TsCl mass ratio range of 1∶1～1∶3 were conducted. Only p-methylphenyl 4,6-o-benzylidene-3-o-p-toluenesulfonyl-1-thio-β-D-glucopyranoside (Ⅱ) was isolated from the product, and its yield was no more than 60%. At the same time, the purification method of Ⅲ has been improved." @default.
- W2357788219 created "2016-06-24" @default.
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- W2357788219 date "2005-01-01" @default.
- W2357788219 modified "2023-09-23" @default.
- W2357788219 title "Study on Synthesis of 2,3-Anhydro-D-glucopyranoside" @default.
- W2357788219 hasPublicationYear "2005" @default.
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