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- W2357960063 abstract "A technique of preparing PdCl2 was from Pd(NH3)2Cl2 by oxidation method was studied. The Pd(NH3)2Cl2 was used as raw material, and was it dissolved in HCl solution. The solution was heated and transformed into(NH4)2PdCl2. Ammonium was removed by oxidation.(NH4)2PdCl2 was transformed into Pd(OH)2 by depositing using NaOH. Pd(OH)2 was filtrated and washed,and then dissolved in HCl solution and was concentrated and crystallized. The research results showed that when dosage of sodium chlorate was 2.48kg, HCl(36%) was 2.75L per kilogram Pd(NH3)2Cl2, concentration of Pd was 20g/L,time of oxidization was 60 minutes, temperature of oxidization was 100℃, pH in depositing Pd was 10, concentration of Pd in depositing Pd was 10g/L, Pd(OH)2 was washed 3 times. The purity of Pd(OH)2 produced by using the technique was over 99.9%,Pd in PdCl2 was over 59.5%, Fe was below 0.002%, NO3- was below 0.02%, total impurity in PdCl2 was below 0.05%. Direct recovery was over 99.9% ." @default.
- W2357960063 created "2016-06-24" @default.
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- W2357960063 date "2005-01-01" @default.
- W2357960063 modified "2023-09-22" @default.
- W2357960063 title "Study on Preparing Palladium Chloride from Pd(NH_3)_2Cl_2 by Oxidation Method" @default.
- W2357960063 hasPublicationYear "2005" @default.
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