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- W2358272007 abstract "OBJECTIVE:To establish the method of determining the blood concentration of pioglitazone hydrochloride. METHODS:Chromatographic column was based on Hypersil C l8 (150mm×4.6mm,5μm),the mobile phase consisted of ace-tonitrile-buffer phosphate(40∶60,V/V)with a flow rate at l.0ml/min,the detecting wavelength was229nm.The blood sample was extracted with dichlormethane.RESULTS:The linear concentration range was25～4000ng/ml(r=0.9998,n=8).The lowest detecting concentration was25ng/ml.The extracting recovery rate of high,medium and low concentrations were(73.33±1.22)%,(76.92±6.57)%and(84.50±3.40)%respectively,the method recovery which were(103.26±3.31)%,(97.31±9.07)%and(99.61±6.48)%respectively.The intra-day RSD4.30%(n=5)and the inter-day RSD8.17%(n=25).CONCLUSION:This method can meet the requirements of both blood concentration determination of pioglitazone hydrochloride and the study of human body pharmacokinetics." @default.
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- W2358272007 date "2005-01-01" @default.
- W2358272007 modified "2023-09-25" @default.
- W2358272007 title "Determination of Blood Concentration of Pioglitazone Hydrochloride by HPLC" @default.
- W2358272007 hasPublicationYear "2005" @default.
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