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- W2358372170 abstract "A microwave-assisted pre-column derivatization-HPLC method was established for the determination of(R)-enantiomer in pregabalin.With microwave-assistance,pregabalin was derivatized with Nα-(5-fluoro-2,4-dinitrophenyl)-D-valine amide as chiral derivatization agent in DMSO.A Hypersil BDS C18 column was used with the mobile phase of 0.1 mol/L ammonium formate solution(adjusted to pH 3.0 with formic acid)-acetonitrile(49︰51) at the detection wavelength of 340 nm.The calibration curve of(R)-enantiomer was linear in the range of 2-20 μg/ml.The LLOQ was 0.24 μg/ml." @default.
- W2358372170 created "2016-06-24" @default.
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- W2358372170 date "2011-01-01" @default.
- W2358372170 modified "2023-09-25" @default.
- W2358372170 title "Determination of(R)-Enantiomer in Pregabalin by HPLC with Microwave-assisted Pre-column Derivatization" @default.
- W2358372170 hasPublicationYear "2011" @default.
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