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• W2358906486 abstract "The intermediate diazidoglyoxime(DAG)was synthesized by one-pot method with glyoxime and NaN3 as starting materials.Then 5,5′-bistetrazole-1,1′-diolate(BTO)was synthesized by reaction of DAG with HCl and Et2 O.The ammonia salt of 5,5′-bistetrazole-1,1′-diolate(ABTOX)was synthesized by metathesis reaction of BTO and NH4 Cl.Its structure was characterized by X-ray single crystal diffractometer.The thermolysis properties of ABTOX were studied by differential thermal analysis/thermogravimetric analysis(DTA/TG),and its impact sensitivity and friction sensitivity were also tested.Results show that the crystal is orthorhombic belonging to space group of Aba2(41)with crystal parameters of the unit cell dimensions as follows:a=1.071 65(13)nm,b=1.070 33(13)nm,c=1.329 04(16)nm,V=1.524 4(3)nm3,z=4,D=1.779g/cm3.The thermal decomposition temperature of ABTOX is 287.8℃ and its impact and friction sensitivities are 46 cm and 0,respectively." @default.
• W2358906486 created "2016-06-24" @default.
• W2358906486 creator A5053367403 @default.
• W2358906486 date "2015-01-01" @default.
• W2358906486 modified "2023-09-23" @default.
• W2358906486 title "Synthesis,Crystal Structure and Properties of the Ammonia Salt of 5,5′-Bistetrazole-1,1′-diolate" @default.
• W2358906486 hasPublicationYear "2015" @default.
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