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- W2358996892 abstract "Objective To obtain the exactly glycosylated peptide by glycosylated N α Fmoc serine and threonine were synthesized as the raw material for solid phase glycopeptide synthesis. Methods The glycosylation of N α Fmoc serine or threonine with 2 acetamido 2 deoxy D galactose(GalNAc) pentaacetate was carried out with BF3 Et2O and SnCl4 as promoters in CH 2Cl 2 or CH 3CN. Results After purification with reversed phase HPLC, the glycosylated N α Fmoc serine or threonine can be further used as the building blocks to synthesize viral or tumorous glycopeptide with solid phase polypeptide synthesizor. Conclusion This method is easy to perform and with high repeatability and better yield, especially the glycosylation is well distributed." @default.
- W2358996892 created "2016-06-24" @default.
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- W2358996892 date "2000-01-01" @default.
- W2358996892 modified "2023-09-25" @default.
- W2358996892 title "Chemical synthesis of building blocks for O linked synthetic glycopeptide" @default.
- W2358996892 hasPublicationYear "2000" @default.
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