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- W2359171616 abstract "Objective: To evaluate the uncertainty of methylergometrine in human plasma determined by HPLC-MS / MS. Methods: The uncertainty caused by various influencing factors in the whole process of determination,including repeatability,balancing,standard solution preparation,drug-spiked plasma,extraction process,the equipment,calibration fitting,and so on. The expanded uncertainty was obtained by calculating each component of uncertainty and the combined uncertainty. Results: The obtained expand uncertainty of 15. 000 ng·mL- 1was 1. 127 ng·mL- 1(P =95%,k =2). Conclusion: The uncertainty determined by HPLC-MS/MS is mainly caused by extraction recovery,solution preparation and the equipment." @default.
- W2359171616 created "2016-06-24" @default.
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- W2359171616 date "2014-01-01" @default.
- W2359171616 modified "2023-09-26" @default.
- W2359171616 title "Uncertainty evaluation in determination of methylergometrine in human plasma by HPLC- MS /MS" @default.
- W2359171616 hasPublicationYear "2014" @default.
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