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- W2359236467 abstract "A facile synthesis of piperonol is reported from catechol. Reacted catechol with excess dichloromethane in an autoclave under nitrogen atmosphere gave 88 4% 1,3-benzodioxole(1), which is directly chlo romethylated to yield 90 1% 5-chloromethyl 1,3-benzodioxole(2) by hydrogen chloride saturated triformol. 2 can easily convert to piperonal by treatment with alcoholic solution of Na 2CO 3 in yield of 97 7%. The total yield is 78%." @default.
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- W2359236467 date "2003-01-01" @default.
- W2359236467 modified "2023-09-25" @default.
- W2359236467 title "Synthesis of Piperonol from Catechol" @default.
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