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- W2359479216 abstract "A synthesis of 3-bromo-2-methoxy-5-nitrophenyl benzyl ether,the aromatic fragment of ansamycin natural product reblastatin,was developed. The key reaction in this synthesis was a Baeyer-Villiger reaction of a benzaldehyde intermediate,as the undesired benzoic acid could be the major product in certain cases. After the optimization of reagents and operation,the desired phenol intermediate was obtained in 84% yield. This approachproduced 3-bromo-2-methoxy-5-nitrophenyl benzyl ether in 5 linear steps and 33% overall yield." @default.
- W2359479216 created "2016-06-24" @default.
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- W2359479216 date "2014-01-01" @default.
- W2359479216 modified "2023-09-27" @default.
- W2359479216 title "Synthesis of 3-bromo-2-methoxy-5-nitrophenyl benzyl ether" @default.
- W2359479216 hasPublicationYear "2014" @default.
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