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- W2359553989 abstract "Objective To establish the method for determination of polysorbate 80 in compound shexiang injection by HPLC-ELSD. Methods It was performed by HPLC-ELSD with TSK GEL G2000SWxl( 7. 8 mm × 300 mm,5 μm) column. Acetonitrile and 0. 01 mol ·L-1ammonium acetate( 8∶ 92) was used as mobile phase,the flow rate was 0. 8ml·min-1,and the temperature was set at 30℃. The evaporated light scattering detector was adopted. The drift tube temperature was 103℃,and the gas flow rate was 2. 5 L·min-1. Results The calibration cueve showed good linearity of polysorbate 80 in the test range from 2. 515 to 100. 6 μg( r = 0. 999 9),and average recovety was 100. 87%( n = 6,RSD = 0. 65%). Conclusion The method is simple,rapid,accurate and reliable,and it can be applied to control the quality of polysorbate 80 in compound shexiang injection." @default.
- W2359553989 created "2016-06-24" @default.
- W2359553989 creator A5036202231 @default.
- W2359553989 date "2014-01-01" @default.
- W2359553989 modified "2023-09-24" @default.
- W2359553989 title "Determination of polysorbate 80 in compound shexiang injection by HPLC-ELSD" @default.
- W2359553989 hasPublicationYear "2014" @default.
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