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- W2359585633 abstract "A zinc complex [Zn(NA)2(H2O)4](Pic)2 was prepared by the reaction of niacinamice and zinc picrate in ethanol water solution, and characterized by elemental analysis and IR spectroscopy. The crystal structure was determined by X-ray diffraction. The crystal crystallizes in the triclinic system, space group P1 with a = 7.050( 1), b = 8.839(3), c= 14.035(3) A, α = 81.16(2),β = 81.92(2). r =66.55(2)°, V= 789.8(3) A3, Z= 1 ,Dc = 1.762g/cm3, F(000) = 428 andμ =0.886 mm-1. The crystal structure was solved by direct methods for the final R = 0.0419 and wR = 0.1094 for 2467 observed reflections with Fo 4σ(Fo). The crystal structure reveals that the zinc ion is trans-octahedral with two pyridyl nitrogens and two aque oxygens at the equatorial positions and two aque oxygens at the axial positions. Every [Zn(NA)2(H2O)4](Pic)2 unit forms twelve hydrogen bonds (of two types: O-H…O and N-H…O) which bridge four [Zn(NA)2(H2O)4](Pic)2 units. The complex forms a three-dimensional network through hydrogen bonds." @default.
- W2359585633 created "2016-06-24" @default.
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- W2359585633 date "2002-01-01" @default.
- W2359585633 modified "2023-09-25" @default.
- W2359585633 title "Preparation and Crystal Structure Investigation of Zinc Picrate Niacinamide" @default.
- W2359585633 hasPublicationYear "2002" @default.
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