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- W2359754286 abstract "In order to establish a method in the determination of AFB1 content in edible vinegar using immune affinity columns,post-column derivation,HPLC and fluorescence detector,combining with immune affinity column and HPLC,the AFB1 content in edible vinegar was analyzed,.The chromatographic conditions included Agilent-C18 column(4.6 mm×300 mm,5 μm) and the mobile phase consisting of a mixture of methanol and water by 65∶35(v/v).The flow rate was 0.8 mL/min.Exciting wavelengh was at 365 nm and emission wavelengh was at 440 nm.The result showed that when the AFB1 content was at 10 ng/ml to 50 ng/ml,the perfect linearity between concentration and peak area ratio was obtained,the recovery rate was 89.36% to 99.19%,and the detection limit was 0.1 μg/kg,the relative standard deviation(RSD) was 1.19% to 5.25%.This method was simple,rapid and accurate with high recovery on the determination of AFB1 content in edible vinegar." @default.
- W2359754286 created "2016-06-24" @default.
- W2359754286 creator A5031417341 @default.
- W2359754286 date "2008-01-01" @default.
- W2359754286 modified "2023-09-24" @default.
- W2359754286 title "Applied research of immune affinity columns-HPLC method on the determination of AFB_1 content in edible vinegar" @default.
- W2359754286 hasPublicationYear "2008" @default.
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