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- W2359817711 abstract "Two porous solid phase microextraction(SPME) fibers were made by C18 bonded silica(C18) and carbon nanotubes(CNTs).The analysis results by electron micrographs indicate that the fiber surface is clinged uniformly and closely.The analytical performances of the two fibers were evaluated by solid-phase microextraction coupling gas chromatography ion trap detector determining phthalate esters(PEs).The two fibers have the same good adsorption properties and precision as the commercial polydimethylsiloxane(PDMS) and polyacrylate(PA) fibers.The mass transfer rate of the analysts is very fast from the sample solution to the fiber when coated with C18 stationary for the large adsorption area and thin coat of C18.It can reach equilibrium in 30 min to both dimethyl phthalate(DMP) and diethyl phthalate(DEP).The concentration factor of middling polarity phthalate esters between C18 stationary phase and sample solution is above 103.The fiber coated CNTs have larger adsorption area and ability,and their capacity are as good as commercial fibers.But they take longer time to reach equilibrium than fiber coated C18." @default.
- W2359817711 created "2016-06-24" @default.
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- W2359817711 date "2008-01-01" @default.
- W2359817711 modified "2023-09-25" @default.
- W2359817711 title "Preparation and characterization of two new fibers for solid phase microextraction" @default.
- W2359817711 hasPublicationYear "2008" @default.
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