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- W2360184310 abstract "A Four-arm initiating core containing 1,3,5-triazine,N,N′-bis-(4,6-dichloro——triazin-2-yl)-ethane-1,2-diamine,was prepared from cyanuric chloride(CNC) and ethylene diamine(EDA) by nucleophilic substitution reaction.The optimum reaction conditions included n(CNC)∶n(EDA)=2∶1,NaOH used as base,n(NaOH)∶n(EDA)=2∶1,dichloromethane and water in volume ratio 1∶1 as solvent,adding rate of aqueous NaOH solution of EDA 1 mL/min,reaction temperature 0～5 ℃ and reaction time 2 h.The product yield reached 95.5%.Structure of the target product was characterized by elementary analysis,MS,~1 HNMR and FTIR." @default.
- W2360184310 created "2016-06-24" @default.
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- W2360184310 date "2007-01-01" @default.
- W2360184310 modified "2023-09-26" @default.
- W2360184310 title "Synthesis and Characterization of a Four-arm Initiating Core Containing 1,3,5-Triazine" @default.
- W2360184310 hasPublicationYear "2007" @default.
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