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- W2360185473 abstract "The solid phase extraction and GC-MS were developed for the determination of 17 organic chlorides and pyrethroid pesticide residues in grain.The organic chlorides and pyrethroid pesticides were extracted from grain samples with petroleum ether,purified by Florisil solid-phase extraction column,and detected by GC-MS with SIM mode(selective ion monitoring).The matrix-matched calibration was used to compensate the matrix effects.The recoveries of 17 pesticide residues ranged from 70.9% to 110.3%.The relative standard deviations were within 2.5%~10.3%.The detection limit was from 1.8μg/kg to 16.8μg/kg." @default.
- W2360185473 created "2016-06-24" @default.
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- W2360185473 date "2010-01-01" @default.
- W2360185473 modified "2023-09-23" @default.
- W2360185473 title "Determination of 17 organic chlorides and pyrethroid pesticide residues in grains by solid-phase extraction and GC-MS" @default.
- W2360185473 hasPublicationYear "2010" @default.
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