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- W2360198731 abstract "[Objective]To establish determination methodology of pentachlorophenol in fish gall bladder by automatic solid-phase microextraction(SPME )with ancillary extraction of supersonic wave and gas chromatography. [Methods]Pentachlorophenol in fish gall bladder was extracted using optimized SPME technology,separated by HP-5 and DB-17 chromatographic columns and the content of pentachlorophenol in fish gall bladder was determined by electron capture detector(ECD ) under optimized conditions.[Results]The linear range of the calibration curve was 0.08-100.00μg/L with a correlation coefficient of 0.9997 and the detection limit for pentachlorophenol was 0.053μg/L.The recovery rates were between 81.5%-92.6%and the relative standard deviations were between 3.6%-6.3%.[Conclusion]The method is simple,rapid and sensitive without solvent pollution,which is a ideal method for determination of pentachlorophenol in fish gall bladder." @default.
- W2360198731 created "2016-06-24" @default.
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- W2360198731 date "2011-01-01" @default.
- W2360198731 modified "2023-09-23" @default.
- W2360198731 title "Determination of Pentachlorophenol in Fish Gall Bladder by Solid Phase Microextraction Gas Chromatography" @default.
- W2360198731 hasPublicationYear "2011" @default.
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