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- W2360445461 abstract "A method was developed for simultaneous determination of pyrrolizidine alkaloids and isoquinoline alkaloids in honey by dispersive solid phase extraction and high performance liquid chromatography-tandem mass spectrometry(QuEChERS-HPLC-MS /MS). The honey samples were extracted with acetonitrile solution and cleaned up with PSA absorbent. Agilent Poroshell 120 SB-C18 chromatographic column was used to separate alkaloids with high sensitivity and satisfactory resolution. The identification and quantification were achieved by using electrospray ionization in positive ion mode( ESI+) with multiple reaction monitoring(MRM). Matrix-matched calibration curves with good correlation coefficients(R2 0. 99) were obtained in the concentration range of 0. 1- 100 μg /L. The recoveries of the spiked samples at 1- 100 μg /kg were in the range of 70% to 110% with the RSD of intra-day and inter-day lower than 15% and 20%,respectively. The limits of detection( LOD) and limits of quantification( LOQ) for all alkaloids were 0. 3 and 1. 0 μg /kg,respectively. This method was successfully applied to the simultaneous determination of pyrrolizidine alkaloids and isoquinoline alkaloids for quantification and confirmation in honey samples." @default.
- W2360445461 created "2016-06-24" @default.
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- W2360445461 date "2014-01-01" @default.
- W2360445461 modified "2023-09-23" @default.
- W2360445461 title "Determination of Alkaloids in Honey by Dispersive Solid Phase Extraction and High Performance Liquid Chromatography-Tandem Mass Spectrometry" @default.
- W2360445461 hasPublicationYear "2014" @default.
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