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- W2360679888 abstract "Ammonium 9-molybdate nickel heteropoly salt with Waugh structure was synthesized by the reaction of nickel sulfate and ammonium heptamolybdate by oxidation of ammonium peroxydisulfate at acetic acid pH4-6.The title compound was characterized by IR,UV-Vis,TG-DT thermal analysis and CV.The fomula was determined by chemical analysis to be(NH4)6[NiMo9O32].8H2O.It can be seen from IR spectrum that there are characteristic band of Waugh-type heteropolyacidic salt in the range of 1000-400cm-1.From UV spectrum,in Ultraviolet region there is a band at 207nm assigned to electronic transition from double bonds of oxygen to Mo atom and there is a bond at 563.2nm in visible range.We can see from the TG-DTA curves that ammonium 9-molybdate nickel heteropoly salt can be decomposed at 1067.9-1103.5K..It indicated from the cyclic voltammetry(CV) curve there was a good linear relationship between ip and v1/2,suggesting the electrode reaction being controlled by diffusion oxido-reduction process.The voltage of cathodic and anodic peak was becoming progressively more positive with decreasing pH,the variation presumably related to variation in protonation.of the cluster." @default.
- W2360679888 created "2016-06-24" @default.
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- W2360679888 date "2008-01-01" @default.
- W2360679888 modified "2023-09-23" @default.
- W2360679888 title "Synthesis and Characterization of Ammonium 9-molybdate Nickel Heteropoly Salt with Waugh Sructure." @default.
- W2360679888 hasPublicationYear "2008" @default.
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