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- W2361204775 abstract "Acetacetic este was refluxed with a solution of Br-2 in CCl-4 for 2 h and then vacuum distillated to give 4-bromo-acetacetic ester in 80.1% yield.A solution of thiourea in alcohol was put into 4-bromo acetacetic ester and then refluxed for 12 h,vacuum distillated to remove alcohol,recrystallized to give ethyl 2-amino-4-methylthiazole-5-carboxylate in 62% yield.It was identified by elemental analysis,FT-IR,(~1 H) NMR and MS." @default.
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- W2361204775 date "2006-01-01" @default.
- W2361204775 modified "2023-09-23" @default.
- W2361204775 title "Synthesis of Ethyl 2-Amino-4-Methylthiazole-5-Carboxylate" @default.
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