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- W2361572246 abstract "OBJECTIVE A method for determination of Imatinib mesylate and related substances was established.METHODS The liquid chromatography was carried out using a Herdera C18(5μm,4.6mm×250mm)column.The mobile phase consisted of methanol-solution of 1-octanesulfonic acid sodium salt(36mmol·L-1),gradient elution.The flow rate was 1mL·min-1.The detection wavelength was 278nm.The injection volume was 20μL.The column temperature was 40℃.RESULTS The intermediates and degraded substances could be separated.Three batches of sample were determined.The calibration curve for Imatinib mesylate was linear in the range of 8~80μg·L-1(r=0.9999).The detection limit for Imatinib mesylate was 0.02μg·mL-1.CONCLUSION The method is specific,accurate,sensitive,simple,and can be used for quality control of Imatinib mesylate." @default.
- W2361572246 created "2016-06-24" @default.
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- W2361572246 date "2012-01-01" @default.
- W2361572246 modified "2023-09-22" @default.
- W2361572246 title "Determination of imatinib mesylate and related substances by gradient elution HPLC" @default.
- W2361572246 hasPublicationYear "2012" @default.
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