Matches in SemOpenAlex for { <https://semopenalex.org/work/W2362151570> ?p ?o ?g. }
Showing items 1 to 65 of
65
with 100 items per page.
- W2362151570 abstract "The process for preparation of seratrodast by condensation reaction from 2,3,5-trimethyl hydroquinone and 7-hydroxy-7-phenylheptanoic acid,which was prepared by chlorination,F-C acidylation,hydrolysis and reduction from ethyl pimelate,was studied.The effects of the molar ratio of reactants and the dosage of catalyst were investigated.The optimum process parameters were determined as follows: molar ratio of ethyl pimelate∶SOCl_2=1∶2.2;7-phenyl-7-oxoheptanoate∶KOH=1∶4;Concentration of KOH 30%;7-hydroxy-7-phenylheptanoic acid∶2,3,5-trimethyl hydroquinone=1∶1.2.7-hydroxy-7-phenylheptanoic acid∶BF_3·Et_2O=1∶1.2.The synthesis of 7-hydroxy-7-phenylheptanoic acid was primarily studied,optimum synthesis conditions were obtained as follows: 7-phenyl-7-oxoheptanoic acid∶KBH_4=1∶1.2,reflux,reaction time 6 h.The total yield of seratrodast was 22.7 %." @default.
- W2362151570 created "2016-06-24" @default.
- W2362151570 creator A5050428915 @default.
- W2362151570 date "2006-01-01" @default.
- W2362151570 modified "2023-09-26" @default.
- W2362151570 title "The process for synthesizing seratrodast" @default.
- W2362151570 hasPublicationYear "2006" @default.
- W2362151570 type Work @default.
- W2362151570 sameAs 2362151570 @default.
- W2362151570 citedByCount "0" @default.
- W2362151570 crossrefType "journal-article" @default.
- W2362151570 hasAuthorship W2362151570A5050428915 @default.
- W2362151570 hasConcept C121332964 @default.
- W2362151570 hasConcept C134121241 @default.
- W2362151570 hasConcept C13965031 @default.
- W2362151570 hasConcept C161790260 @default.
- W2362151570 hasConcept C178790620 @default.
- W2362151570 hasConcept C185592680 @default.
- W2362151570 hasConcept C191897082 @default.
- W2362151570 hasConcept C192562407 @default.
- W2362151570 hasConcept C200093464 @default.
- W2362151570 hasConcept C2777550763 @default.
- W2362151570 hasConcept C2994067411 @default.
- W2362151570 hasConcept C94412978 @default.
- W2362151570 hasConcept C97355855 @default.
- W2362151570 hasConceptScore W2362151570C121332964 @default.
- W2362151570 hasConceptScore W2362151570C134121241 @default.
- W2362151570 hasConceptScore W2362151570C13965031 @default.
- W2362151570 hasConceptScore W2362151570C161790260 @default.
- W2362151570 hasConceptScore W2362151570C178790620 @default.
- W2362151570 hasConceptScore W2362151570C185592680 @default.
- W2362151570 hasConceptScore W2362151570C191897082 @default.
- W2362151570 hasConceptScore W2362151570C192562407 @default.
- W2362151570 hasConceptScore W2362151570C200093464 @default.
- W2362151570 hasConceptScore W2362151570C2777550763 @default.
- W2362151570 hasConceptScore W2362151570C2994067411 @default.
- W2362151570 hasConceptScore W2362151570C94412978 @default.
- W2362151570 hasConceptScore W2362151570C97355855 @default.
- W2362151570 hasLocation W23621515701 @default.
- W2362151570 hasOpenAccess W2362151570 @default.
- W2362151570 hasPrimaryLocation W23621515701 @default.
- W2362151570 hasRelatedWork W2351558273 @default.
- W2362151570 hasRelatedWork W2353531919 @default.
- W2362151570 hasRelatedWork W2354534878 @default.
- W2362151570 hasRelatedWork W2354994148 @default.
- W2362151570 hasRelatedWork W2358274971 @default.
- W2362151570 hasRelatedWork W2364649249 @default.
- W2362151570 hasRelatedWork W2366111887 @default.
- W2362151570 hasRelatedWork W2368463608 @default.
- W2362151570 hasRelatedWork W2371876160 @default.
- W2362151570 hasRelatedWork W2374038301 @default.
- W2362151570 hasRelatedWork W2374483621 @default.
- W2362151570 hasRelatedWork W2378564986 @default.
- W2362151570 hasRelatedWork W2380763287 @default.
- W2362151570 hasRelatedWork W2383845499 @default.
- W2362151570 hasRelatedWork W2384016182 @default.
- W2362151570 hasRelatedWork W2387117436 @default.
- W2362151570 hasRelatedWork W2392452734 @default.
- W2362151570 hasRelatedWork W2774287961 @default.
- W2362151570 hasRelatedWork W2836063149 @default.
- W2362151570 hasRelatedWork W2876466139 @default.
- W2362151570 isParatext "false" @default.
- W2362151570 isRetracted "false" @default.
- W2362151570 magId "2362151570" @default.
- W2362151570 workType "article" @default.