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- W2362169174 abstract "Intercalated montmorillonite(M MT) was fabricated by co-intercalation of dodecyl dimethyl benzyl ammonium chloride and tetraethoxysilane.Compared with natural MMT, the specific surface area of intercalated MMT was greatly increased.The intercalated MMT was used to modify expanded graphite, and thus a novel MMT modified expanded graphite electrode was obtained.Aniline was determined at the modified electrode by differential pulse voltammetry.The results showed that the intercalated MMT modified expanded graphite electrode could significantly enhance the charge transfer rate of aniline and the oxidation peak current of aniline was greatly improved at this modified electrode. The intercalated MMT modified expanded graphite electrode showed a linear response range between 10 and 1 000 μm ol/L of aniline with a correlation coeffcient of 0.9969, and the detection limit was calculated as 6.05 μm ol/L( S/N=3).Five intercalated MMT modified expanded graphite electrodes were used to determine 1.0 mmol /L aniline, and the RSD was calculated to be 3.83%.Blank spiked recovery experiments were carried out and the recoveries were in the range of 96%-101%." @default.
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- W2362169174 date "2012-01-01" @default.
- W2362169174 modified "2023-09-25" @default.
- W2362169174 title "Electro-catalytic Oxidation and Determination of Aniline Based on a Novel Montmorillonite Modified Expanded Graphite Electrode" @default.
- W2362169174 hasPublicationYear "2012" @default.
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