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- W2362181801 abstract "Four 3,5-disubstituted isoxazoline derivatives(4a~4d)in good yields(84%~95%)were synthesized by 1,3-dipolar cycloaddition of soluble poly(ethylene glycol)(PEG)-supported acrylate with nitrile oxides generated in situ from aldoximes,and then releasing from the PEG using NaOCH3-CH3OH.The structures were characterized by 1H NMR,IR and EI-MS.The crystal structure of 4d was determined by X-ray single-crystal diffraction.The 4d belongs to monolinic system,space group C2/c with a=26.965 5(17),b=9.370 5(6),c=8.946 5(6),α=γ=90°,β=97.226(2)°,V=2 242.6(3)3,Z=8,Dc=1.299 mg·m-3,μ=0.094 mm-1,F(000)=928,R1=0.041 5,wR2=0.106 4." @default.
- W2362181801 created "2016-06-24" @default.
- W2362181801 creator A5052385519 @default.
- W2362181801 date "2009-01-01" @default.
- W2362181801 modified "2023-09-23" @default.
- W2362181801 title "Liquid-phase Synthesis and Crystal Structure of Poly(ethylene glycol)-supported Isoxazoline Derivatives" @default.
- W2362181801 hasPublicationYear "2009" @default.
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