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- W2362519536 abstract "The fingerprint of raw milk based on high performance liquid chromatography-mass spectrometry (HPLC-MS) in negative ion mode was established to evaluate the quality of raw milk. The raw milk was extracted by acetonitrile and the obtained constituents were eluted by acetonitrile and 0.1% acetic acid solution with a gradient program at a column temperature of 30 ℃ within 85 min. A total of 11 common peaks had been identified. The methodology was investigated by the relative peak area and relative retention time with No. 7 peak as the reference. The results showed that the fingerprint established by this method has reasonable reproducibility with the relative standard deviations (RSDs) less than 0.79% for the relative retention time and less than 2.84% for the relative peak area. Based on the fingerprint,a labelling HPLC-MS spectrogram was obtained for the screening of hazards by adding several representative hazards,such as benzoic acid etc. An amount of 50 pure milk samples in Shenyang supermarkets were inspected,and preliminary results had been achieved." @default.
- W2362519536 created "2016-06-24" @default.
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- W2362519536 date "2010-01-01" @default.
- W2362519536 modified "2023-09-23" @default.
- W2362519536 title "Establishment of high performance liquid chromatographic fingerprint of raw milk" @default.
- W2362519536 hasPublicationYear "2010" @default.
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