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- W2362598692 abstract "OBJECTIVE To eastablish a method for the determination of residual organic solvents in Sulfasalazine raw material by the use of GC.METHODS The GC determination was performed on a glass column which was packed 10% PEG-20M/102 with FID detection.The injection port and detector temperature were 180℃ and 200℃ respectively.RESULTS Under experiment condition,acetone had good linear relationship between 0.817～8.18 mg·mL-1,RSD% of middle precision∶1.8%.Methylbenzene had good linear relationship between 0.1732～1.732mg·mL-1,RSD% of middle precision∶1.6%.Every component was separated thoroughly.Three batches of samples were analyzed by the method.None of residual organic solvent was found to exceed quality limit.CONCLUSION The method is proved to be accurate and sensitive.It is suitable for the analysis of the residual organic solvents in sulfasalazine." @default.
- W2362598692 created "2016-06-24" @default.
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- W2362598692 date "2008-01-01" @default.
- W2362598692 modified "2023-09-23" @default.
- W2362598692 title "Determination of residual organic solvents in Sulfasalazine by GC" @default.
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