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- W2362685305 abstract "Objective:To develop a HPLC-MS method for determination of ibudilast in human plasma. Methods: Phenacetin was used as an internal standard and the chromatographic conditions adopted were:Lichrospher C18 column(250mm×4.6mm,5μm) ,a mobile phase of 0.5% acetic acid-methanol(20:80) with a flow rate of 1.0mL·min-1, using a single quadrapole MS as detector, Re-sults: Ibudilast had a good linear range of 2-200ng·mL-1 ( r = 0.999 7) with a detection limit of 1.0 ng·mL-1. The average recovery was 99.37 % with an extraction recovery of more than 95 % . RSD was less than 5% for intra-day and inter-day assay. Conclusion: The method established is simple, rapid, sensitive,accurate and suitable for determination of ibudilast in human plasma." @default.
- W2362685305 created "2016-06-24" @default.
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- W2362685305 date "2004-01-01" @default.
- W2362685305 modified "2023-09-24" @default.
- W2362685305 title "Determination of ibudilast in human plasma by HPLC-MS" @default.
- W2362685305 hasPublicationYear "2004" @default.
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