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- W2362985205 abstract "Sample of fish(2.0 g) was treated by MSPD extraction(with 10 mL of CH3CH),homogenized for 1 min by mixing at a rate of 6 000 r·min-1,and then mixed with 4 g of anhydrous MgSO4 and 1.5 g of NaCl.The mixture was centrifuged for 3 min at a rate of 5 000 r·min-1.One mL of the supernatant was mixed with 50 mg each of N-propyl-ethylene diamine and C18 powder.The mixture was centrifuged for 3 min at a rate of 10 000 r·min-1 and 0.5 mL of supernatant was mixed with 0.5 mL of water and analyzed by HPLC-MS/MS under prescribed conditions.Tests for recovery were made by addition of mixed standard solution at 3 concentration levels to matrixes of 3 kinds of fishes,giving results of recovery in the ranges of 83.7%-93.2% for praziquantel and 85.2%-92.8% for propargite,with values of RSD′s(n=5) ranged from 3.7% to 9.3% and 2.1% to 9.6% respectively.Values of detection limits(3S/N) were found same as 0.3 μg·kg-1." @default.
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- W2362985205 date "2011-01-01" @default.
- W2362985205 modified "2023-09-24" @default.
- W2362985205 title "HPLC-MS/MS Determination of Praziquantel and Propangite in Fish with Sample Treatment by Matrix Solid Phase Dispersion Extraction" @default.
- W2362985205 hasPublicationYear "2011" @default.
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