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- W2363065323 abstract "In a cationic membrane electrolytic cell, 4-aminopyridine was synthesized by constant potential of cathode technique and the process conditions were optimized. Its cyclic voltammetry shows that there exist quite a number of unstable intermediates during the electroreduction of 4-nitropyridine 1-oxide. Under the optimal conditions, which are as follows: granular lead used as cathode, Ti-base lead dioxide as anode and calomel electrode as reference electrode, the water solution of 4-nitropyridine-1-oxide with pH=3 and 1% mass concentration as cathodic electrolyte and the solution of sulfuric acid with 10% mass concentration as anodic electrolyte, ammonium sulfate as supporting electrolyte, supplying 200% theoretic electric quantity and the temperature at 50℃, the 88.2% electrolyses yield of 4-aminopyridine and 44.1% current efficiency can be reached respectively. This green synthesis technology, characterized by simple process and high yield, is expected to instead ferrous reduction, which pollutes environment seriously." @default.
- W2363065323 created "2016-06-24" @default.
- W2363065323 creator A5045538484 @default.
- W2363065323 date "2005-01-01" @default.
- W2363065323 modified "2023-09-27" @default.
- W2363065323 title "Process Research on the Electrosynthesis of 4-Aminopyridine" @default.
- W2363065323 hasPublicationYear "2005" @default.
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