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- W2363190391 abstract "OBJECTIVE To establish a method based on nonaqueo us capillary electrophoresis for the separation of Z ,E isomers of doxepine hydrochloride.METHODS The separation was performed on a fuse d silica capillary of 50 μm×47 cm (40 cm of effective length), and the runnin g buffer was methanol acetonitrile (95∶5) containing 200 mmol·L -1 ammon ium acetate and 3.0% glacial acetic acid.Samples were injected by pressure mode. The applied voltage was 25 kV and the detection wavelength was set at 254 nm.RESULTS The method was validated in terms of reproducibility,l inearity,recovery,limits of quantitation and detection.CONCLUSION The method appeared to be simple and fast for the separation of Z ,E isomers of doxepine hydrochloride." @default.
- W2363190391 created "2016-06-24" @default.
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- W2363190391 date "2002-01-01" @default.
- W2363190391 modified "2023-09-25" @default.
- W2363190391 title "Determination of doxepin hydrochloride isomers by nonaqueous capillary electrophoresis" @default.
- W2363190391 hasPublicationYear "2002" @default.
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