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- W2363216960 abstract "A method of sol-gel for preparing a W/WO_3 pH electrode was presented. H~+ response characteristics, such as response range, response sensitivity, response time were investigated. The effect of heat-treatment on response linear relation was discussed. The influences of interfered ions and solution temperatures were also taken into consideration. Many kinds of determination technology, such as TG, DSC, IR, SEM, AFM,XPS, XRD were used to characterize the film. The results show that the film appears in crack dried-mud, and the film is composed of WO_3, WO_3·H_2O or WO_3·0.33H_2O; the hydrate water decreases with the increase of the heat-treatment temperature; the W~+6 in the electrode film transfers to W~+5 in the course of H~+ response; the H~+ response course is controlled by the H~+ diffusion from the solution to the WO_3 crystalline, which is indicated in the EIS spectra; the best heat-treatment temperature is 200℃, and at this temperature, the electrode has an H~+ response sensitivity of 52mV/pH." @default.
- W2363216960 created "2016-06-24" @default.
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- W2363216960 date "2005-01-01" @default.
- W2363216960 modified "2023-09-25" @default.
- W2363216960 title "Preparation and H~+ response mechanism of W/WO_3 pH electrode by sol-gel method" @default.
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