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- W2363533704 abstract "Poly(N,N-diethylacrylamide) with a terminal hydroxyl end group(PDEAm-OH) was synthesized by radical polymerization in the presence of 2-mercaptoethanol(ME).Thermosensitive poly(N,N-diethylacrylamide)(PDEAm) macromonomer was prepared by condensation reaction of PDEAm-OH with acryloyl chloride.The macromonomer was characterized by FT-IR,1H NMR,UV-spectrophotometer,which has a lower critical solution temperature(LCST) of 36.4℃ in aqueous media.Then PDEAm grafted poly(acrylonitrile/styrene)(PDEAm-g-PAN/PSt) polymeric microspheres can be prepared by dispersion copolymerization of PDEAm macromonomer with AN/St in ethanol/water mixed solvents.The morphology and the average size of the polymeric microspheres can be controlled by changing the polymerization conditions.Scanning electron microscopy(SEM) images and particle size analysis under different temperature show that the microspheres have monodispersibility and thermosensitivity." @default.
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- W2363533704 date "2012-01-01" @default.
- W2363533704 modified "2023-09-22" @default.
- W2363533704 title "Preparation and characterization of poly(N,N-diethyl acrylamide)-g-polyacrylonitrile/polystyrene microspheres with thermosensitivity" @default.
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