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- W2363773834 abstract "A highly sensitive,specific and credible method for the simultaneous determination of 20 anabolic steroids in urine of pig performed by GC/MS was developed.Samples of urine of pig(10.0 g)were deconjugated by Helix pomatia juice,extracted with acetonitrile,cleaned-up through dual columns of C18 and NH2,the extracts obtained were derivatized with heptafluorobutyric anhydride,following formation of the di-heptafluorobutyryl(di-HFB)derivative,and then identification and quantification were carried out by capillary gas chromatography-mass spectrometry.For quantitation,the external standards were used and the method was validated with blank samples fortified at 0.5,2.5 and 2.5 μg/kg with 10.0 g sample.The detection limits were less than 0.25 μg/kg for all analytes.Overall recovery and repeatability(relative standard deviations,RSD)ranged from 77.0% to 111.0%,and from 4.3% to 23.2%,respectively." @default.
- W2363773834 created "2016-06-24" @default.
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- W2363773834 date "2009-01-01" @default.
- W2363773834 modified "2023-09-25" @default.
- W2363773834 title "Determination of Multi-residue of Anabolic Steroids by Gas Chromatography-Mass Spectrometry" @default.
- W2363773834 hasPublicationYear "2009" @default.
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