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- W2363876504 abstract "A new method for the determination of N-methylcarbamate pesticides using lauric acid surfactant and ammonia as buffer by micellar electrokinetic chromatography-electrospray ionization mass spectrometry was developed.The samples were separated by an uncoated capillary(75μm×83 cm) on the operating voltage of 25 kV using 30 mmol/L lauric acid-120 mmol/L ammonia mixture containing 25% acetonitrile(pH 9.5) as the running buffer and 70% 2-propanol solution(containing 2 mmol/L acetic acid) as the sheath liquid.The baseline separation of seven compounds was achieved with satisfactory repeatability and sensitivity.The detection limit of each analyte varied from 0.080 to 0.18 μg/L with the preconcentration of AccuBOND-NH2 solid phase extraction column.The average recoveries of seven analytes from farm waste water ranged from 87.2% to 93.8% with relative standard deviations in the range of 2.9%~8.5%.The method is simple,rapid,accurate and suitable for the simultaneous determination of these herbicides in waste water." @default.
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- W2363876504 date "2012-01-01" @default.
- W2363876504 modified "2023-09-25" @default.
- W2363876504 title "Simultaneous determination of N-methylcarbamate pesticides in farm water by micellar electrokinetic chromatography-electrospray ionization mass spectrometry" @default.
- W2363876504 hasPublicationYear "2012" @default.
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